The temperature measurement plays a decisive role in organic synthesis. Synthos 3000 provides a dual solution for precise temperature control.
Synthos 3000
Microwave technology
Synthos 3000 delivers 1400 W of continuous, unpulsed microwave power via two magnetrons, therefore ensuring a highly homogeneous microwave field. This enables effective heating rates for large reaction volumes and optimum reproducibility for any synthesis. Efficient stirring
Sufficient mixing is essential for organic syntheses, especially on a large scale. Synthos 3000 has a powerful magnetic stirrer which provides for efficient mixing in every single reaction vessel and therefore ensures:
• Better conversion rates
• Improved yield
• Shorter reaction times
• Simplified work-up of products
High performance rotors
The rotors used in Synthos 3000 are specially designed for high pressure applications. Their high safety standards allow for the development of even the most difficult reactions. Temperatures up to 300 °C and pressures up to 80 bar open new dimensions in chemical processing.
Fast reactions
Employing higher temperatures leads to drastically reduced reaction times and the efficiency of the synthesis can be significantly increased. Development which usually requires days or weeks can now be completed in hours as the individual reaction steps only take a few minutes.
Reliable safety concept
Using chemicals in the microwave field always involves risk, especially with large volumes. The reliable safety system of the Synthos 3000 has multiple step, active and passive protection elements which minimize the dangers of spontaneous reactions. This guarantees the highest level of safety for the user at any time.
Automatic rotor detection prevents misuse at unsuitable conditions
High pressure stability (up to 120 bar) of utilized vessels
Metal safety disks protect pressure vessels from explosions
Software-aided pressure rate control
Self-acting cooling and exhausting system
Double-check temperature control protects magnetrons from overheating
Exact control of exothermic reactions by IR and inside temperature measurement
Microwave synthesis platform Synthos 3000 - efficient, powerful and robust
Rotor systems for different applications
Rotor 16 is the perfect tool for a number of organic reactions up to 1L reaction volume or up to 16 parallel reactions. The rotor is equipped with 100 mL PTFE-TFM liners. The controlled operating pressure of the reaction vessels (MF100 and HF100) can be increased from 20 to 40 bar by simple exchanging of the pressure jackets.
The temperature measurement plays a decisive role in organic synthesis. Synthos 3000 provides a dual solution for precise temperature control.
• Automatic rotor detection prevents misuse at unsuitable conditions
• High pressure stability (up to 120 bar) of utilized vessels
• Metal safety disks protect pressure vessels from explosions
• Software-aided pressure rate control
• Self-acting cooling and exhausting system
Employing higher temperatures leads to drastically reduced reaction times and the efficiency of the synthesis can be significantly increased.
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